Case study of failure analysis of oxide-based all-solid-state batteries.

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We present a case study of a series of analyses conducted to identify failure points and perform cross-sectional observations on an oxide-based all-solid-state battery that was destroyed during reliability testing. Thermal analysis revealed a tendency for strong heat generation on the side, and X-ray transmission observations showed white linear contrast anomalies near the boundary where heat generation was observed in the X-ray transmission image. It is suspected that some abnormalities may have occurred in the white line area. When CP cross-sectional SEM observations were conducted on the areas where anomalies were visible, layer delamination was observed. It is inferred that delamination occurred between the current collector and electrolyte layers due to the expansion and contraction of the positive (negative) electrode layers during reliability testing. 【Case Overview】 ■ Sample Information: Oxide-based all-solid-state battery that experienced degradation due to charge and discharge testing ■ Thermal Analysis Results: A tendency for strong heat generation on the side was observed ■ Other Analysis Contents: - X-ray transmission observation - CP cross-sectional observation and elemental analysis via SEM *For more details, please refer to the PDF document or feel free to contact us.

Batteries and Capacitors