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  4. Analysis of mica sheet adhesive components using GC/MS.
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  • Dec 06, 2023
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Dec 06, 2023

Analysis of mica sheet adhesive components using GC/MS.

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This is an introduction to the analysis of mica sheet adhesive components using GC/MS. To investigate what components are contained in the mica sheet, spectroscopic measurements were conducted, suggesting that a silicone-based adhesive is used. To determine the composition of the silicone-based adhesive, GC/MS measurements were performed. It was found that pentacyclooctasiloxane is used, and it was also revealed that dibutyl phthalate is added as a plasticizer and linear saturated hydrocarbons such as tridecane are added as lubricants.
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Analysis of mica sheet adhesive components using GC/MS.

It is possible to investigate components that cannot be identified by spectroscopy alone, as well as trace additives that cannot be detected!

We will introduce the analysis of the components of mica sheet adhesive using GC/MS. To investigate what components are contained in the mica sheet, spectroscopic measurements were conducted, suggesting the use of silicone-based adhesives. To examine the composition of the silicone-based adhesive used, GC/MS measurements were performed. It was found that pentacyclooctasiloxane is used, and it was also discovered that plasticizers such as dibutyl phthalate and chain-saturated hydrocarbons like tridecane are added as lubricants. [Mica Sheet Components] ■ Pentacyclooctasiloxane (cage-like polymethylsilsesquioxane) ■ Dibutyl phthalate ■ Chain-saturated hydrocarbons such as tridecane *For more details, please refer to the PDF document or feel free to contact us.

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GCMS analysis of liquid crystal components

Comparison of components in liquid crystal panels using gas chromatography-mass spectrometry (GC-MS) is published!

This document introduces a comparison of components in PC monitors and digital clocks using gas chromatography-mass spectrometry (GC-MS). Liquid crystal displays contain small organic substances (liquid crystal molecules). These have evolved into molecular structures suitable for product characteristics due to technological innovations. Our company clarifies these differences at the molecular level using GC-MS, allowing us to confirm that the liquid crystal molecules are appropriate for their intended use and to check for the presence of impurities. [Contents] ■ Comparison of components in PC monitors and digital clocks using GC-MS ■ Case studies of GC-MS analysis of liquid crystal components We compared the number of components and characteristics of segment-type liquid crystal displays (digital clocks) and color TFT liquid crystal displays (PC monitors). *For more details, please refer to the PDF document or feel free to contact us.

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Identification of natural components by GCMS

Focusing on sandalwood (byakudan), which is used as a raw material for incense! Here is an example of component analysis using GC-MS.

Due to the risk of depletion of natural ingredients, artificially synthesized alternative components may be used, and their identification is suitable through separation and analysis methods such as GCMS. This time, we focused on sandalwood (Byakudan), which is used as a raw material for incense. We tested whether the components of sandalwood could be detected in two types of incense (A and B) with sandalwood scent. In incense A, santanol was detected, whereas in incense B, santanol was not detected, and another aromatic component was found. Among these, bugdanol is a type of synthetic fragrance, and due to its structural characteristics, it is believed to have a sandalwood-like scent. [Components of Incense A] ■ Bugdanol: Trace amount ■ Cedrol: None ■ α-Santalol: Present ■ β-Santalol: Present *For more details, please refer to the PDF document or feel free to contact us.

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Analysis of impurities in organic solvents

The aldol reaction progresses under the influence of temperature, humidity, and light! Example of impurity analysis in ethanol and acetone.

This is an example of analyzing impurities detected in a solvent when stored in inappropriate conditions. Ethanol, which was stored in a light-protective reagent bottle in a cool, dark place, was transferred to a used plastic wash bottle and left at room temperature for about a month. As a result, impurities such as triethyl borate and alkylbenzenes were detected. Additionally, acetone stored in a light-protective reagent bottle in a cool, dark place was transferred to a transparent glass bottle without light protection and left at room temperature for about a month, resulting in the detection of diacetone alcohol as an impurity. [Impurity Analysis in Ethanol] - Ethanol stored in a light-protective reagent bottle in a cool, dark place was transferred to a used plastic wash bottle and left at room temperature for about a month (the wash bottle was not sealed as the opening was exposed). - Result: Impurities such as triethyl borate and alkylbenzenes were detected. *For more details, please refer to the PDF document or feel free to contact us.*

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[Information] GC-MS Analysis Device Guide

Introducing the sample introduction device and the types of analytical samples and analysis that each device specializes in!

GC-MS analysis is a method commonly used for the analysis of organic components and organic structure analysis. With auxiliary devices, it can accommodate a wide range of analyses, from low molecular substances like solvents to high molecular substances like plastics. This document introduces the sample introduction devices owned by Aites, as well as the types of analysis samples and analysis content that each device specializes in. Please take a moment to read it. 【Contents】 ■ Overview ■ Conditions ■ Samples ■ Data Obtained ■ Analysis Examples *For more details, please refer to the PDF document or feel free to contact us.

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[Data] Analysis of Additive Defects in Polymers by Thermal Desorption GC-MS

It is possible to analyze with high sensitivity using thermal desorption GC-MS analysis! We propose methods tailored to the symptoms of malfunctions and your objectives.

Various additives are used in polymers to improve stability and processability; however, due to environmental impact and long-term storage, additive components may precipitate on the polymer surface, or the additives themselves may undergo chemical changes, leading to discoloration and degradation. This document presents examples of analyses conducted using thermal desorption GC-MS to examine the bleed-out of additives and the chemical changes of additive components due to UV irradiation. Although additive components are present in small quantities compared to the main polymer components, they can be analyzed sensitively using thermal desorption GC-MS. We propose methods tailored to specific issues or objectives, such as predicting product degradation in combination with reliability testing, thermal analysis, and main component analysis, so please feel free to contact us. [Contents] ■ Analysis of additive components that bled out from nitrile rubber ■ Analysis of additive components in nylon 66 subjected to UV irradiation *For more details, please refer to the PDF document or feel free to contact us.

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Analysis of difficult-to-detect substances by reaction thermal decomposition GC-MS.

By adding a special reagent to the sample and heating it, it becomes possible to detect substances that are usually difficult to detect!

In a typical thermal decomposition GCMS, samples are heated to detect volatile components, but it is difficult to analyze components that do not volatilize upon heating or those with low detection sensitivity. Therefore, by adding a special reagent to the sample and heating it, it becomes possible to detect substances that are usually difficult to identify. For example, in the analysis of polymers, thermal decomposition of the polymer results in the detection of a large number of decomposition products, and in some cases, peaks may overlap with other additives, making analysis challenging. However, by performing reactive thermal decomposition GCMS, it is possible to detect the monomer methyl ester and to separate and analyze it from the additives. Thus, even when the target analyte is difficult to detect using conventional analysis, reactive thermal decomposition GCMS allows for sensitive detection by selecting appropriate reagents for the analyte. [Examples] - Analysis of phthalate esters (DIDP) - Analysis of polymers (polyethylene terephthalate) - Analysis of copper corrosion inhibitors (BTA) *For more details, please refer to the PDF document or feel free to contact us.

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Related catalog(7)

Analysis of mica sheet adhesive components using GC/MS.

Analysis of mica sheet adhesive components using GC/MS.

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Identification of natural components by GCMS.

Identification of natural components by GCMS.

TECHNICAL
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Analysis of impurities in organic solvents

Analysis of impurities in organic solvents

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[Information] GC-MS Analysis Device Guide

[Information] GC-MS Analysis Device Guide

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Analysis of Additive Defects in Polymers Using Thermal Desorption GC-MS

Analysis of Additive Defects in Polymers Using Thermal Desorption GC-MS

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Analysis of difficult-to-detect substances using reaction thermal decomposition GC-MS.

Analysis of difficult-to-detect substances using reaction thermal decomposition GC-MS.

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GCMS analysis of liquid crystal components

GCMS analysis of liquid crystal components

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[Free Materials Available] Introducing Useful Information on Vehicle Detection Sensors!

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To customers considering the introduction of vehicle detection sensors for parking lot construction, design, or management: Are you facing any challenges with current issues or selecting the right sensors for parking management? Hotron offers free materials that explain how to utilize vehicle detection sensors and the benefits of their introduction! ▽ Here is the lineup of materials ◉ Vehicle Detection Sensor Basic Guide This guide focuses on the challenges and solutions in parking lot operations, introducing the overview of vehicle detection sensors. ◉ Key Points for Introducing Vehicle Detection Sensors This material discusses the benefits of introduction based on installation locations and specific challenges. ◉ Case Studies of Vehicle Detection Sensor Implementation This document presents the challenges before implementation and the results after introduction. For more details, please download from our website and check it out. https://www.hotron.co.jp/download/

Nov 14, 2025

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[Special Selection] Nanoe X for Commercial Use! Evolved Panasonic Commercial Air Conditioners - Built-in All-Duct Type / Ceiling Built-in Cassette Type | Suminomori

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Starting from October 2025, Panasonic's indoor units for office and store air conditioners will be renewed! In this renewal, all models will come standard with "100 times nanoe X." This not only enhances comfort with commercial air conditioning but also contributes to improving air quality. Additionally, improvements in installation efficiency to enhance on-site work productivity and a strengthened lineup to accommodate diverse spaces have been implemented. The new indoor units are equipped with high concentrations of nanoe X as standard! They demonstrate a high effectiveness in purifying indoor air during air conditioner operation, providing a safer and more comfortable environment for office and store users and employees. Furthermore, the center of the suction inlet and the center of the hanging bolt have been unified. This allows for the combined use of canvas ducts and panels, improving installation efficiency. If you have any questions or would like a quote, please feel free to contact us. We will fully support you in replacing your commercial air conditioning!

Nov 14, 2025

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採用イベント「Kort Valuta Night」11/26開催!

“Kort Valuta Night” Recruitment Event in November — A Chance to Hear Real Voices from Our Team Casually get to know Kort Valuta — several participants have already joined the company after attending!

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Kort Valuta Inc. (Head Office: Shibuya, Tokyo; CEO: Hideki Shibata) is pleased to announce that we will hold our next recruitment event, “Kort Valuta Night,” on November 26, 2025. This recurring event offers an opportunity for potential candidates to casually learn about our company culture and team atmosphere before applying. By lowering the barrier to entry and providing authentic insights from current employees, the event helps participants gain a more concrete sense of what it’s like to work at Kort Valuta. Since the event’s launch, approximately ten attendees have gone on to join the company in a range of roles — including marketing, customer support, and backend engineering.

Nov 13, 2025

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I have received the "Climate Change Action Minister's Award."

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Our company has been awarded the "Minister of the Environment Award for Climate Change Action for Fiscal Year 2025." This award is presented annually by the Ministry of the Environment to honor individuals and organizations that have made significant contributions to the mitigation and adaptation of climate change. Our efforts to balance energy conservation and comfort through "Akarina," as well as the initiatives we have undertaken together with the companies that have adopted it, have been recognized. We sincerely thank everyone who has supported and adopted Akarina for their invaluable assistance.

Nov 13, 2025

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Start of offering the vehicle passage time prediction system "MS-VPP" using microwave sensors.

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We are pleased to announce the development of the vehicle passage time prediction system "MS-VPP," which measures the speed of vehicles approaching construction sites using microwave sensors and informs the predicted passage time through signage and tablets. This system will be available to construction contractors starting in November 2025. ■Product Overview - "MS-VPP" detects vehicles approaching construction sites and measures their speed using microwave sensors, displaying the vehicle speed and the predicted passage time at specified locations on signage and tablets. It can also measure and display data for vehicles passing continuously. - The data control panel connected to the microwave sensor transmits the vehicle speed data and calculated passage prediction time via LTE. By utilizing microwave sensors, it enables accurate detection and speed measurement of vehicles even at night or in bad weather, and since data processing occurs on the receiving side without going through the cloud, information can be displayed without any time lag. - As a result, drivers of construction vehicles exiting from construction entrances and workers directing traffic can understand "how many seconds until a vehicle passes near the site entrance," thereby implementing safety measures in areas with poor visibility.

Nov 13, 2025

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