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マイクロトラック・ベル

capital6580Ten thousand
number of employees120
addressOsaka/Suminoe-ku, Osaka-shi/2-52, Higashi 8-chome, Nangang
phone06-6655-0362
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last updated:Jun 12, 2023
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Sample analysis and demonstration

If you are considering purchasing the device, we will respond free of charge!

At Microtrack Bell, we are accepting "sample analysis and demonstrations" at any time. Please check the measurement accuracy through sample analysis and the operability through demonstrations. We also welcome inquiries regarding measurements. If you are considering purchasing the equipment, we will provide our services free of charge. Additionally, we also offer paid sample analysis. Please feel free to contact us. For the "analysis items," please see below. *For more details, please refer to the related links or feel free to contact us.*

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[Online Technical Seminar] Measurement Technology for Evaluating the Properties of Powders and Granules

Particle size distribution from nanometers to micrometers / Particle shape from micrometers to millimeters.

This document is the presentation material from the webinar "Powder Processing and Particle Characterization Techniques Using Bead Mills" held on Wednesday, May 19, 2021. It includes the MRB product lineup (particle size distribution and particle shape), as well as information on particle size and scattering patterns, changes in particle size with grinding time, and measurement results from SYNC. It introduces particle size distributions from nanometers to micrometers and particle shapes from micrometers to millimeters. [Contents (excerpt)] ■ MRB product lineup (particle size distribution and particle shape) ■ Integration of SYNC-LD (MT3300EX II) and DIA (SI) ■ Point 1: Continuous detection of 150 particles with 3 lasers ■ Case of laser diffraction scattering method (LD) (data differences) ■ Differences in optical systems of laser diffraction scattering method (LD) *For more details, please refer to the PDF document or feel free to contact us.

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[Webinar] Product Introduction and Key Points to Know Before Budget Application

Established the new business brand "MICROTRAC MRB"! Featuring spray particle size distribution measurement devices, etc.! (2021 edition)

This document introduces MRB products for the 2021 budget application. With the aim of providing customers with a one-stop solution through outstanding technology in powder and particle evaluation, we have established a new business brand, "MICROTRAC MRB." We feature devices such as the spray particle size distribution measurement device "AEROTRAC II," the particle shape and size distribution measurement device "CAMSIZER M1," and the specific surface area/porosity distribution measurement device "BELSORP MINI X." We encourage you to read it. [Contents (excerpt)] ■ Microtrac Bel Corp ■ Product lineup ■ Evaluation items and content for materials ■ MRB product lineup (particle size distribution and shape) ■ Static image analysis and dynamic image analysis *For more details, please refer to the PDF document or feel free to contact us.

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Fundamentals of BET Surface Area and Pore Distribution Evaluation by Gas Adsorption Isotherm Measurement (5)

[Web Seminar] Nitrogen Adsorption Isotherm Measurement and Micropore Evaluation! Providing methods for accurate measurement and analysis.

Various functional materials (porous and non-porous) are utilized in multiple fields such as the environment, energy, pharmaceuticals, and the aerospace industry, making the characterization of these materials essential. In particular, the specific surface area and pore distribution obtained through gas adsorption methods are among the important data in material development. This seminar, aimed at beginners, will provide an overview of the necessity of adsorption evaluation in each application, an outline of adsorption measurement, and analytical methods using adsorption measurements based on JIS (z-8830, 8831-2, 3) and ISO (9277, 15901-2, 15901-3), along with explanations of terminology, to offer correct measurement and analysis methods. *For more details, please refer to the PDF materials or feel free to contact us.

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[Data] Evaluation of pore structure of porous materials using NLDFT method and GCMC method.

Evaluation of pore structure of porous materials with cylindrical pores using NLDFT and GCMC methods - Selection of suitable adsorbates and analysis methods?

So far, various methods for evaluating the pore structure of porous materials have been used based on the differences in pore structures. In the micro-pore region, methods such as the HK method, SF method, and CY method based on adsorption potential theory have been employed, while in the meso-macro pore region, classical pore distribution analysis methods such as the INNES method and BJH method based on capillary condensation theory have been used. On the other hand, in recent years, there has been growing attention on new pore distribution analysis methods such as NLDFT and GCMC, which allow for analysis based on a unified theory from micro-pores to meso-macro pores through computer simulations. This document examines which theory, NLDFT or GCMC, is more suitable for pore distribution analysis. Additionally, while the adsorbate proposed by IUPAC 2015 is Ar adsorption, it also investigates the usefulness of N2 adsorption. Specifically, it analyzes the N2 and Ar actual adsorption isotherms of mesoporous silica MCM41, MFI, and MTW zeolites. *For more details, please refer to the PDF document or feel free to contact us.*

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[Data] Evaluation of Pore Structure of Activated Carbon Fiber by GCMC Method

Publication on the evaluation of pore structure of activated carbon fibers with slit-type micropores using the GCMC method.

In the document regarding the evaluation of pore structures of porous materials with cylindrical pores using the NLDFT method and GCMC method, it was stated that GCMC appropriately evaluates pore diameter and pore volume compared to NLDFT, using cylindrical pores as a case study. In this document, the pore structure evaluation of activated carbon fibers with slit-shaped pores was conducted using the GCMC method, and based on these results, a discussion on pore shape models was carried out. Please take a moment to read it. *For more details, please refer to the PDF document or feel free to contact us.*

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[Web Seminar] Handling and Measurement of "Foundry Sand"

Reduction, sieving, particle size distribution, particle shape! For those already involved in casting and those who want to learn about it in the future.

With the advancement of high functionality in cast products, the demands for surface smoothness, filling density, and strength of molds have become more sophisticated, making the characteristics of the casting sand that composes the molds extremely important. This time, we will introduce measurement techniques for handling casting sand, as well as screening and dynamic image analysis. [Seminar Content] ■ Classification and reduction of casting sand ■ Measurement technology of particle size distribution and particle shape using dynamic image analysis CAMSIZER ■ Case studies on particle size distribution and particle shape measurement of casting sand *For more details, please refer to the PDF materials or feel free to contact us.

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[Web Seminar] Powder Processing and Particle Characterization Techniques Using Bead Mills

Introducing synchronized measurement technology, unique fine particle measurement techniques, and examples of measuring raw materials and nanoparticles!

Electrodevices, including precision instruments utilized in various industries such as IoT, energy, and the environment, are required to be both high-performance and compact. To achieve product miniaturization, the breakdown of raw materials is essential, and the powder processing technology represented by bead mills, specifically "grinding and dispersion," is a very important factor. Additionally, appropriately evaluating that the particles after processing have the desired particle size distribution is necessary in a wide range of scenarios, from research and development to quality control. In this seminar, we will introduce examples of dispersion into new fine particles from Aishizawa Fine Tech Co., Ltd., along with our company's innovative synchronization measurement technology and unique fine particle measurement technology, including measurement examples of raw materials and nanoparticles, as well as points to consider during measurement. [Seminar Content] ■ Lecture 1: New fine particle size reduction examples using wet and dry bead mills ■ Lecture 2: "Measurement" technology for evaluating the characteristics of powders ■ Demonstration: "Measurement" technology for powders ■ Q&A session *For more details, please refer to the PDF document or feel free to contact us.

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Fundamentals of BET Surface Area and Pore Distribution Evaluation by Gas Adsorption Isotherm Measurement (4)

[Web Seminar] Nitrogen Adsorption Isotherm Measurement and Mesopore Evaluation! Providing methods for accurate measurement and analysis.

Various functional materials (porous and non-porous) are utilized in a wide range of fields such as the environment, energy, pharmaceuticals, and the aerospace industry, making the characterization of these materials essential. In particular, the specific surface area and pore distribution obtained through gas adsorption methods are among the important data in material development. Therefore, this seminar will target beginners and provide an overview of the necessity of adsorption evaluation in each application, an outline of adsorption measurement, and analytical methods using adsorption measurements, along with explanations of terms based on JIS (z-8830, 8831-2, 3) and ISO, to offer correct measurement and analysis methods. *For more details, please refer to the PDF materials or feel free to contact us.

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Structural evaluation of PCP/MOF and zeolites using gas adsorption methods.

[Web Seminar] Lecture by Professor Masakazu Higuchi from Kyoto University iCeMS! Structural Evaluation of PCP/MOF and Zeolites by Gas Adsorption Method

With the advancement of various material developments, porous functional materials are increasingly attracting attention in the energy and environmental fields. In this webinar, we introduced the fundamentals of material evaluation using gas adsorption methods, which are essential for the characterization of porous coordination polymers (PCP/MOF) and zeolites, both of which are gaining attention as new porous materials. We also presented case studies on structural evaluation using new pore distribution analysis theories such as GCMC and DFT. Additionally, we invited Professor Masakazu Higuchi from Kyoto University's iCeMS, who is at the forefront of PCP/MOF research, to discuss the research trends and commercialization prospects of these materials. *For more details, please refer to the PDF document or feel free to contact us.*

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Handling and characterization of "all-solid-state battery materials"

[Web Seminar] For those who are already involved in solid-state batteries, as well as for those who want to learn about them from now on!

All-solid-state batteries," for which research and development aimed at practical application is accelerating, involve processes such as ball milling, heat treatment, gas analysis, particle size distribution, particle shape, specific surface area, pore distribution, true density, and surface characteristics. They are attracting significant attention as secondary batteries with CO2 reduction, high safety, and large capacity and high output. Since all the battery constituent materials are solid, methods for sample preparation that enhance the compactness of the materials themselves and between the materials, as well as evaluation methods, are becoming increasingly important. This time, we will focus on grinding (ball milling) in material synthesis and measurement techniques for powder properties. [Seminar Content] ■ Retsch (Väder Scientific Co., Ltd.) - Grinding machine (ball mill) ■ Microtrac Bel Corp. - Specific surface area, pore distribution, true density, surface characteristics, particle size distribution, particle shape evaluation *For more details, please refer to the PDF document or feel free to contact us.

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Fundamentals of BET Surface Area and Pore Distribution Evaluation by Gas Adsorption Isotherm Measurement (3)

[Web Seminar] Structural Evaluation of Various Materials Using the t-plot Method! Introduction to Planar Adsorption Theory and More.

Various functional materials (porous and non-porous) are utilized in multiple fields such as the environment, energy, pharmaceuticals, and the aerospace industry, making the characterization of these materials essential. In particular, the specific surface area and pore distribution obtained through gas adsorption methods are among the important data in material development. Therefore, this seminar will target beginners and provide an overview of the necessity of adsorption evaluation in each application, an outline of adsorption measurement, and analytical methods using adsorption measurements, incorporating explanations of terms based on JIS (z-8830, 8831-2, 3) and ISO, to offer correct measurement and analysis methods. *For more details, please refer to the PDF materials or feel free to contact us.

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Handling and property evaluation of construction materials such as cement and concrete.

[Web Seminar] For those who are already involved in building materials, as well as those who want to learn from now on!

The powder characteristics of raw materials (cement, aggregates, fly ash, and other additives) used in construction materials such as concrete and mortar are very important, as they significantly influence the strength and durability of structures like stadiums, apartments, highways, bridges, and dams. In this seminar, we will introduce handling techniques for cement and aggregates, including particle size reduction and sieving, as well as evaluation techniques for the physical properties of powder materials. [Seminar Content] ■ Letcher (Wader Scientific Co., Ltd.) - Particle size reduction, sieving, electric furnace ■ Microtrack Bell Co., Ltd. - Particle size distribution, particle shape, specific surface area, pore distribution, true density, surface characteristics *For more details, please refer to the PDF document or feel free to contact us.

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Fundamentals of BET Surface Area and Pore Distribution Evaluation by Gas Adsorption Isotherm Measurement (2)

[Web Seminar] What can we learn from nitrogen adsorption isotherm measurements? An introduction to adsorption measurement overview and specific surface area evaluation.

Various functional materials (porous and non-porous) are utilized in multiple fields such as the environment, energy, pharmaceuticals, and the aerospace industry, making the characterization of these materials essential. In particular, the specific surface area and pore distribution obtained through gas adsorption methods are among the important data in material development. Therefore, this seminar will target beginners and provide an overview of the necessity of adsorption evaluation in each application, the basics of adsorption measurement, and analytical methods using adsorption measurements, along with explanations of terms based on JIS (z-8830, 8831-2, 3) and ISO, to offer correct measurement and analysis methods. *For more details, please refer to the PDF materials or feel free to contact us.

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Fundamentals of BET Surface Area and Pore Distribution Evaluation by Gas Adsorption Isotherm Measurement

[Web Seminar] Nitrogen Adsorption Isotherm Measurement and BET Surface Area Evaluation! Introduction to the Differences Between Multi-Point Method and Single-Point Method.

Various functional materials (porous and non-porous) are utilized in multiple fields such as the environment, energy, pharmaceuticals, and the aerospace industry, making the characterization of these materials essential. In particular, the specific surface area and pore distribution obtained through gas adsorption methods are among the important data in material development. This seminar is aimed at beginners and will provide an overview of the necessity of adsorption evaluation in various applications, an outline of adsorption measurement, and analytical methods using adsorption measurements, incorporating explanations of terms based on JIS (z-8830, 8831-2, 3) and ISO (9277, 15901-2, 15901-3), to offer correct measurement and analysis methods. *For more details, please refer to the PDF materials or feel free to contact us.

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Proposal of various gas adsorption measurement and analysis methods utilizing and applying CO2 adsorption.

[Web Seminar] Introduction to suitable adsorbents for various applications and purposes!

As the first installment of the 2021 Microtrac MRB webinar, we will introduce the evaluation methods for pore structure using common N2 and Ar adsorption, along with the ultra-micropore evaluation of electrode materials such as Li-ion batteries through CO2 adsorption, and the evaluation of separation materials targeting CCS and CCUS (adsorption rate, breakthrough curve). We will explain the evaluation methods and features using porous carbon and zeolites, incorporating actual measurement data. Additionally, we will introduce suitable adsorbates based on each application and purpose. *For more details, please refer to the PDF materials or feel free to contact us.*

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[Web Seminar] Metal Additive Manufacturing Technology and Evaluation Techniques for Materials and Fabricated Products

For those who are already engaged in metal additive manufacturing technology, as well as for those who want to learn about it in the future!

The manufacturing using metal additive manufacturing technology (commonly known as 3D printing) is widely spreading in Europe, particularly in Germany. This seminar focused on "evaluation techniques for materials and molded products," presenting a perspective that has not been explored before. We introduced new information, including trends in international standards, and invited Professor Hideki Kyogoku, a specially appointed professor at Kinki University and project leader of the Technical Research Association for Next-Generation 3D Additive Manufacturing Technology (TRAFAM), to give a lecture. 【Program】 ■ Keynote Speech: Professor Hideki Kyogoku, Specially Appointed Professor, Next-Generation Fundamental Technology Research Institute, Kinki University ■ Classification and reduction of metal powders ■ Measurement of particle size distribution and particle shape of metal powders ■ Stress relief, debinding, and sintering of additive manufactured parts ■ Elemental analysis of metal powders and additive manufactured products ■ Sample production for structural analysis of molded parts: cutting to polishing *For more details, please refer to the PDF document or feel free to contact us.

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[Web Seminar] Fundamentals of Solid Catalyst Evaluation Using Gas Adsorption Method

Evaluation of solid catalyst active sites / Evaluation of carbon functional groups and metal oxides / Precious metal catalysts / CO2 breakthrough curve

Solid catalysts are utilized in various fields such as the environment and energy, making the characterization of these materials essential. In this seminar, we will introduce measurement and analysis methods using gas adsorption techniques to understand the active sites, active surface area, and reaction behavior of various solid catalysts and catalyst supports, along with measurement data and evaluation instruments. [Content] ■ Evaluation methods for solid catalysts using gas adsorption ■ Measurement overview (flow method, pulse method, constant volume method) ■ Evaluation of active sites, reactivity, oxidation, and reduction using temperature-programmed spectroscopy (zeolites, metal oxides, carbon black) ■ Evaluation of precious metal catalysts using pulse measurement methods ■ Evaluation of separation performance using breakthrough curve method (CO2 separation, two-component adsorption separation, CCSU) - Reference: BET single-point method for specific surface area evaluation - MicrotracMRB catalyst evaluation instruments: BELCAT II/BELMASS/BELMETAL 3/BELREA *For more details, please refer to the PDF document or feel free to contact us.

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What are the suitable theories and adsorbates for evaluating the pore structures of porous carbon and silica?

[Web Seminar] Introduction to the Theory of Suitable Pore Distribution Evaluation and What Adsorbates Are.

In the Microtrac MRB Webinar Series 1 and 3, we introduced the points to consider in adsorption isotherm measurements, the BET specific surface area evaluation method, and classical pore structure evaluation (such as the t-method, capillary condensation theory, and adsorption potential theory). This time, using porous carbon, silica, and zeolites, which are used in various battery electrodes, gas separation, catalysts, and catalyst support materials, we will present an overview of the new pore distribution evaluation theory (NLDFT/GCMC) and from these evaluation cases, we will introduce what constitutes an appropriate pore distribution evaluation theory and adsorbate. Additionally, we will introduce the breakthrough curve measurement, which has been added as a new feature to the catalyst evaluation device "BELCAT II," along with measurement examples for single-component and two-component cases. *For more details, please refer to the PDF materials or feel free to contact us.

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[Web Seminar] Frontiers of Particle Characterization Analysis through Image Analysis

Introducing examples of powder and particle analysis made possible by image analysis, including "CAMSIZER"!

We will introduce new technologies for static and dynamic image analysis methods for particle shape and particle size measurement, along with various case studies of property analysis for different powders and granules using these methods. Additionally, we will also introduce the image analysis particle shape and particle size measurement device "CAMSIZER." [Examples of measured particles and applications] ■ Ceramics: abrasives, building materials, cement ■ Carbon fibers: automotive parts, plastic molded products ■ Metal particles: metal 3D printing, metal powder injection molding, solder, carbide tools ■ Granules: solid formulations, food ■ Emulsions: resins, rubber ■ Glass beads: light-reflecting materials ■ Agglomerated particles, contaminant particles: case studies of powder and granule analysis made possible by image analysis *For more details, please refer to the PDF document or feel free to contact us.

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[Web Seminar] Evaluation of Pore Structure of Porous Carbon and Silica

An explanation of pore structure evaluation obtained from gas adsorption isotherms, incorporating an overview of various analytical theories and measurement examples!

Porous carbon used for various battery electrode materials, conductive additives, and catalyst materials, along with silica, will be discussed in terms of pore structure evaluation obtained from gas adsorption isotherms, incorporating an overview of analytical theories and measurement examples. Specifically, we will introduce evaluation methods for the specific surface area inside and outside the pores and the capacity of each pore (planar adsorption theory), as well as classical methods for evaluating micropore and mesopore distribution (capillary condensation theory, adsorption potential theory), including graphical representations. Additionally, we will introduce the high-precision gas/vapor adsorption measurement device "BELSORP MAXII-HP/HV." [Seminar Content] ■ Pore structure evaluation obtained from gas adsorption isotherms ■ Introduction of "BELSORP MAXII-HP/HV" ■ Introduction of applications/markets *For more details, please refer to the PDF document or feel free to contact us.

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Adsorption isotherm measurement and specific surface area evaluation of porous and non-porous carbon materials.

[Web Seminar] Providing excellent solutions for various applications along with high customer service!

In 2020, Microtrac Bell (Japan), Microtrac (USA), and Microtrac Retsch (Germany) launched a new brand called "Microtrac MRB." As the first installment of a webinar series to mark the launch of the new brand, we will introduce the BET method for evaluating specific surface area obtained from adsorption isotherm measurements, focusing on porous and non-porous carbon used in various battery electrode materials and conductive additives. [Webinar Content] ■ Title: Adsorption Isotherm Measurement and Specific Surface Area Evaluation of Porous and Non-Porous Carbon Materials ■ Presentation Content - What is an adsorption isotherm? Information obtained from it, the process of conducting adsorption isotherm measurements, and points to note - What is the BET specific surface area obtained from adsorption isotherms? Points to consider during evaluation with examples of carbon materials *For more details, please refer to the PDF document or feel free to contact us.

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Image analysis particle shape and particle size distribution measurement device "CAMSIZER"

[Web Seminar] The Truth About Particle Characteristics Revealed Through Image Analysis. Particle Size, Particle Shape, and True Property Analysis with CAMSIZER!

Various particle measurement devices are available, including sieving, laser diffraction/scattering, centrifugal sedimentation, and dynamic light scattering methods. Each has its advantages, but they also have limitations and constraints in their measurement principles or methods, often making it difficult to understand the essential particle characteristics. To address this issue, we introduce the image analysis-based particle shape and particle size distribution measurement device "CAMSIZER." Thanks to the transparent image analysis technology, the true nature of the particles can be revealed. 【Seminar Content】 ■ Static image analysis type "CAMSIZER M1" ■ Dynamic image analysis types "CAMSIZER X2" and "CAMSIZER P4" - Introduction of various particle measurement examples using these image analysis devices - Measurement cases that can be understood through image analysis Examples: Food (crystals, granules), pharmaceuticals, metal powders, sand, ceramics, fibers, etc. *For more details, please refer to the PDF document or feel free to contact us.

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[Web Seminar] Synchronization Analysis of Particle Characteristics

Laser diffraction and scattering method + dynamic image analysis method! Introducing various case studies of property analysis of powders and granules using SYNC.

The standard laser diffraction and scattering particle size distribution measurement device has evolved further. Introducing the new measurement technology of SYNC: "Laser diffraction and scattering + dynamic image analysis particle size distribution and particle shape measurement device," along with various case studies of property analysis of powders and granules by SYNC. *For more details, please refer to the PDF document or feel free to contact us.

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Evaluation of Raw Material Properties and Product Quality in Metal Additive Manufacturing and Metal Powder Injection Molding

[Web Seminar] Introducing new technologies and products related to particle size distribution, particle shape, heat treatment, cutting, polishing, and hardness testing!

Microtrac MRB Co., Ltd. held a commemorative webinar to mark the launch of its new brand "MicrotracMRB." Following the first session titled "Introduction to BET Surface Area Evaluation Method and New Product BELSORP MAXG," this time, in collaboration with our group company, Varda Scientific Co., Ltd., we will focus on metal additive manufacturing (AM) that achieves the production of complex-shaped metal parts with high precision and strength, as well as metal injection molding (MIM). We will introduce new technologies and products related to the evaluation of raw material properties (particle size distribution and particle shape) and the inspection of processed products (heat treatment, cutting, polishing, and hardness). [Seminar Content] ■ On particle size distribution and shape evaluation - Koji Sato, Sales Promotion Department, Microtrac MRB Co., Ltd. ■ On heat treatment, cutting, polishing, and hardness testing - Hiroshi Takatsuji, President, Varda Scientific Co., Ltd. *For more details, please refer to the PDF materials or feel free to contact us.

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No. 37 Evaluation of Metal Dispersion of Au-supported Catalysts

A detailed introduction to specific methods and precautions for evaluating the metal dispersion of Au-supported catalysts!

Gold-supported catalysts are used in important industrial reactions such as selective oxidation, selective hydrogenation, and water-gas shift reactions, and are known to be very useful catalysts, albeit in a limited capacity. However, even when conducting metal dispersion measurements using the pulse method, which is crucial for evaluating metal-supported catalysts, CO and H2 do not adsorb at room temperature, making accurate evaluation impossible. This document discusses the specific methods and precautions for evaluating the metal dispersion of gold-supported catalysts through CO pulse measurements at low temperatures around -100°C. We encourage you to read it. 【Contents】 ■ Overview ■ Measurement ■ Summary *For more details, please refer to the PDF document or feel free to contact us.

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No. 36 Steam Treatment Method in NH3-TPD

A detailed explanation of the specific methods and precautions for steam treatment, which is considered effective for the removal of l-peaks!

Characterization of solid acid catalysts represented by zeolites is frequently conducted using the measurement of acidity through temperature-programmed desorption of ammonia. In this method, it is often observed that the spectrum exhibits two peaks, l (low temperature) and h (high temperature). The l-peak is attributed to ammonia that is further hydrogen-bonded to the NH4+ cation at the acid site and is not considered to indicate acidity. This document provides a detailed description of the specific methods and precautions for steam treatment, which is said to be effective in removing the l-peak. We encourage you to read it. [Contents] ■ Overview ■ Experiment ■ Summary *For more details, please refer to the PDF document or feel free to contact us.

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No. 35 Measurement of Metal Dispersion of Cu-Supported Catalysts by N2O Pulse Measurement

Introducing specific methods and precautions for measuring metal dispersion using the N2O pulse method!

The measurement of metal dispersion using CO or H2 pulse adsorption methods is a widely applicable technique for measuring the metal dispersion of various metal-supported catalysts. However, there are many metal-supported catalysts where the probe molecules CO and H2 do not adsorb, making the measurement of metal dispersion in those cases difficult. The N2O pulse method is a measurement technique that utilizes the oxidation reaction of surface metals rather than adsorption, and it can be used for catalysts that support metals that are relatively easy to oxidize (such as Cu). This document provides a detailed description of the specific methods and points to note regarding metal dispersion measurement using the N2O pulse method. We encourage you to read it. [Contents] ■ Overview ■ Measurement ■ Summary *For more details, please refer to the PDF document or feel free to contact us.

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Measurement of Adsorption Heat of MFI Zeolite in No.34 NH3-TPD Measurement

Detailed information on specific methods and precautions for measuring acidity using TPD!

Solid acid catalysts represented by zeolites are applied in many fields as industrial catalysts, and their research is also conducted widely. To understand the solid acid catalytic action, it is necessary to characterize the surface acidity, and the measurement of acidic properties (acid amount, acid strength [adsorption heat]) through temperature-programmed desorption of ammonia is widely used as a method. This document provides a detailed description of the specific methods and points of caution regarding the measurement of acidic properties using TPD. We encourage you to read it. [Contents] ■ Overview ■ Experiment ■ Summary *For more details, please refer to the PDF document or feel free to contact us.

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No.33 Measurement of Metal Dispersion in Precious Metal Catalysts

Introduction to the principles and measurement methods of pulse metal dispersion measurement! Examples of measurements for general precious metal-supported catalysts are included.

Metal-supported catalysts are essential in many industrial reactions, and research is actively being conducted to enhance their functionality and efficiency. Methods for measuring metal dispersion include differential adsorption measurements of CO or H2, and measurements of the amount of chemisorption using CO or H2 pulses. The pulse adsorption method is particularly suitable for rapid characterization due to its short measurement time. This document provides a detailed discussion on pulse metal dispersion measurement using the catalyst analysis device "BELCAT." We encourage you to read it. [Contents] ■ Overview ■ Experiment ■ Conclusion *For more details, please refer to the PDF document or feel free to contact us.

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No.32 Measurement of Thermal Reduction of Metal Oxides

Introduction to the principles and measurement methods of temperature-programmed reduction (TPR) measurements! Examples of measurements of common metal oxides are provided.

One of the important methods for characterizing transition metal-based supported catalysts, which are widely used regardless of being organic or inorganic and can be oxidized or reduced at relatively low temperatures, is temperature-programmed reduction (TPR) measurement. By conducting TPR measurements on supported metal oxides and measuring their reduction temperatures, it is possible to determine the reduction treatment temperature during the adjustment stage of metal catalysts and to establish the upper usage temperature of metal oxide catalysts under reducing atmospheres. This document provides a detailed description of TPR measurements using the catalyst analysis device "BELCAT." We encourage you to read it. [Contents] ■ Overview ■ Experiment ■ Summary *For more details, please refer to the PDF document or feel free to contact us.

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No. 31 Suitable Preprocessing Conditions for H2 Pulse Measurement

Discussion on standard measurement conditions for H2 pulse measurement! Recommended pretreatment conditions for H2 pulse measurement are also included.

The evaluation of the dispersion of metal-supported catalysts is generally conducted through CO or H2 pulse adsorption measurements. H2 has a weaker adsorption strength to precious metals compared to CO, and depending on the support, it may cause spillover phenomena, which is why it is not often chosen. However, due to its low toxicity and constant stoichiometric ratio, there are cases where H2 is used for pulse adsorption measurements. When H2 pulse measurements are conducted under the same conditions as CO pulse measurements, significantly lower dispersion may be obtained compared to CO pulse measurements. This document examines the causes of this phenomenon and its countermeasures, and reports on the standard measurement conditions for H2 pulse measurements. [Contents] ■ Overview ■ Experiment ■ Results and Discussion *For more details, please refer to the PDF document or feel free to contact us.

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No.30 Measurement of Metal Dispersion in Carbon Noble Metal Supported Catalysts

Conducted CO pulse measurements at a pretreatment temperature of 100°C! Photos of the sample changes after the measurement are included!

Catalysts that carry a large amount of platinum group metals (such as Pt and Ru) on carbon supports are used in the fuel cell MEA (membrane/electrode assembly) for the fuel electrode (negative electrode) and air electrode (positive electrode), and research is actively being conducted to improve efficiency and CO poisoning resistance. The dispersion evaluation of these carbon-supported precious metal catalysts can generally be performed using CO pulse methods; however, in some cases, it may be chosen not to perform oxygen pretreatment to avoid the combustion of the carbon support, leading to variations in measurement conditions among researchers. This document provides a detailed discussion on the effects of oxygen treatment on pulse metal dispersion measurements using the catalyst analysis device "BELCAT," as well as recommended measurement conditions. [Contents] ■ Overview ■ Experiment ■ Summary *For more details, please refer to the PDF document or feel free to contact us.

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No.29 Evaluation of the specific surface area of CB using the BET method

Implemented using the flow method! Measuring the BET specific surface area of carbon black using "BELCAT"!

This document introduces the evaluation of the BET surface area of carbon black (CB) using the BET single-point method. We will measure the BET surface area of carbon black (M11-02) using "BELCAT" (flow method). As a pre-treatment, M11-02 was placed in a sample tube, which was then connected to the connector port on the heater side. After flowing 30% N2/He, the heater was heated to 305°C and maintained for 2 hours, followed by cooling down to room temperature. The results are explained in detail using graphs. We encourage you to read it. 【Contents】 ■ Overview ■ Experiment ■ Results *For more details, please refer to the PDF document or feel free to contact us.

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No. 28 Hydrogen TPR Measurement of CuO by BELCAT

A method for evaluating the reducing properties of catalysts using hydrogen! An explanation of hydrogen TPR measurements for CuO!

This document introduces the hydrogen TPR measurement of CuO using "BELCAT." TPR stands for Temperature Programmed Reduction (Reaction) and is used to evaluate the reducibility of catalysts with hydrogen. In the experiment, the change in the concentration of hydrogen gas in the carrier gas during heating or the amount of reaction products is recorded as a function of time or temperature. In this case, the equipment for TPD can be used almost as is, but if a TCD is used as the detector, an H2O trap must be placed before the detector. [Contents] ■ Overview ■ Experiment and Results ■ References *For more details, please refer to the PDF document or feel free to contact us.

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No.27 Measurement of Pulsed Chemical Adsorption - Evaluation of Metal Dispersion Degree -

Explanation of the results from experiments conducted with "BELCATII"! Examples of parameters in chemical adsorption measurements are provided!

Metal-supported catalysts play an important role in industrial processes such as hydrogenation, dehydrogenation, and isomerization reactions. In these metal-supported catalysts, an increase in the dispersion of the metal not only increases the number of active sites effective for the reaction but also enhances the contribution of atoms at the corners and edges of the metal particles, leading to changes in reaction activity and selectivity due to the interactions between the metal and the reactants. Therefore, understanding the metal dispersion is very important in the case of metal catalysts. This document introduces the evaluation of metal dispersion using "pulsed chemical adsorption measurement." We encourage you to read it. 【Contents】 ■ Overview ■ Experiment ■ Results ■ References *For more details, please refer to the PDF document or feel free to contact us.

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No. 26 Heating Rate Desorption Measurement - Evaluation of Desorption Energy and Adsorption Heat -

Explanation of temperature-programmed desorption measurement (NH3-TPD) using numerous graphs! Includes pre-treatment and measurement programs for the experiment!

Acidic zeolites have acidic sites on their surface that significantly influence their catalytic activity. Knowing the strength and quantity of these acidic sites is essential for the evaluation of acidic zeolites, and methods such as calorimetry and ammonia TPD have been used to determine these properties. This document provides a detailed explanation of the evaluation of desorption energy and adsorption heat in "Temperature Programmed Desorption Measurement (NH3-TPD)." We encourage you to read it. 【Contents】 ■ Overview ■ Experiment ■ Results ■ References *For more details, please refer to the PDF document or feel free to contact us.

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Rapid Surface Area Measurement Device (6 Samples Continuous) 'BELSORP MR6'

Demo/analysis now accepting. Additional sample measurements can also be conducted at the sample exchange station!

The "BELSORP MR6" is a fully automated rapid BET evaluation system that can continuously measure up to 6 samples from pretreatment to measurement and BET specific surface area calculation. By continuously performing pretreatment, cooling, and measurement of samples, it is possible to efficiently complete the entire process in about half the time compared to conventional products for 6 sample measurements. With the sample exchange station, new samples can be swapped in during measurement, allowing for additional sample measurements. 【Features】 ■ Measurement range (0.01m² and above) ■ Short measurement time (15 minutes per measurement, including calibration) ■ Excellent reproducibility achieved through automatic capture of temperature and pressure during calibration ■ Low specific surface area measurement using Kr adsorption *For more details, please refer to the PDF document or feel free to contact us.

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Rapid Surface Area Measurement Device (1 Sample) 'BELSORP MR1'

Demo/analysis now available. Just a 15-minute BET evaluation! It's a very user-friendly device, especially for users with little experience.

The "BELSORP MR1" is a high-efficiency, high-precision standalone rapid BET surface area measurement device that can simultaneously perform sample pretreatment and measurement. The specific surface area of materials is measured using the BET single-point method. With high-sensitivity measurements using a thermal conductivity detector (TCD), thermometer, and pressure gauge, measurement results can be obtained in approximately 15 minutes, including calibration. 【Features】 ■ High-sensitivity thermal conductivity detector (with auto-zero function) ■ High-precision measurements through temperature and pressure measurements ■ Measurement results and trend data can be saved to a USB flash memory ■ Compact design that does not require an external PC ■ Low specific surface area measurement using Kr *For more details, please refer to the PDF document or feel free to contact us.

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Low Temperature Variable Temperature Control Unit "BELCRYO"

It can be used in a wide range of applications, such as the evaluation of gas storage materials like hydrogen!

"BELCRYO" is a low-temperature variable temperature control unit that can perform adsorption isotherm measurements at various temperatures from cryogenic to high temperatures. When using refrigerants for temperature control in adsorption, there were limitations on measurement time, but it allows for long-duration measurements without concern. It supports simultaneous measurements with optical instruments (such as XRPD and SAXS) and simultaneous measurements of gas adsorption behavior and structural changes. 【Features】 ■ Temperature adjustment is possible from 50K to 473K within 0.01K ■ Standard cell (2cm³) and small capacity cell (0.5cm³) are available ■ Enables automatic measurements in combination with the BELSORP MAX series ■ Up to 3 samples can be measured simultaneously ■ High-pressure measurements (0.9MPa) with BELSORP MAX II-HP ■ N2, CO2, O2, H2, HCs, CO, and other inert gases *For more details, please refer to the PDF document or feel free to contact us.

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Preprocessing device "BELPREP VAC Series"

Demo/Analysis now available. We offer two models with different sample processing capacities to meet your needs!

To perform accurate adsorption isotherm measurements, it is necessary to degas the sample. This pretreatment can be carried out using a dedicated heater in the adsorption measurement device itself or with a separate pretreatment device, the "BELPREP VAC series." The sample is pretreated by vacuum heating or inert gas flow heating. We offer two models, "BELPREP VAC II" and "BELPREP VAC III," with different numbers of samples processed according to customer requirements. 【Features】 ■ Samples are pretreated by vacuum heating or inert gas flow heating ■ Pretreatment and measurement can be performed simultaneously ■ Two models with different sample processing capacities are available *For more details, please refer to the PDF materials or feel free to contact us.

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Analysis software "BELMaster"

Demo/Analysis now available. Easy and highly efficient! Equipped with a routine analysis setting function that is convenient during analysis. It is effective when performing the same analysis each time.

"BELMaster" is an analysis software that implements a variety of analysis programs, including specific surface area, pore distribution, adsorption heat, and adsorption rate. With drag-and-drop functionality for adsorption isotherm measurement data, various data analyses can be easily performed. It is equipped with a routine analysis setting feature that is convenient for performing the same analysis each time. Based on years of experience, it provides sophisticated advanced analysis theories, allowing anyone to easily and efficiently execute the analysis program for sample characteristic evaluation. 【Features】 ■ Implements a variety of analysis programs ■ Analysis results can be output in Excel format via drag-and-drop ■ Equipped with a routine analysis setting feature for convenience in performing the same analysis each time ■ Unique registration of reference isotherms such as t-plot and αs plot analysis is possible *For more details, please refer to the PDF materials or feel free to contact us.

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BELSORP Series Measurement Software

Demo/Analysis now available! Guides provided for each software setting item! Easy to use even for inexperienced users.

The "Measurement Software" prioritizes usability and is equipped with many features to enhance labor productivity. The BELSORP series includes numerous functions, making it important to develop software that simplifies usage. It guides users step by step through several procedures, such as executing measurements and preparing before measurements. This user-friendly feature allows even inexperienced users to utilize it easily. 【Features】 ■ Common GUI (compatible with BELSORP MINI X, MAX G, MAX II) ■ Simple mode and professional mode available according to user experience ■ Three measurement modes available: - High-precision mode for research and development - Multi-sample measurement mode for quality control - Rapid BET measurement mode for high throughput *For more details, please refer to the PDF materials or feel free to contact us.

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BELSORP Series Options and Accessories

Demo/analysis currently available. Options such as "heater & controller" and "protective cover" are available!

We would like to introduce the "Options and Accessories" of our "BELSORP Series." Starting with "standard consumables" necessary for adsorption isotherm measurement, such as sample cells and volume reduction rods, we also offer options like "Heater & Controller," "Protective Cover," and "Gas Selector." Please feel free to contact us when you need assistance. 【Features of Standard Consumables】 ■ Standard consumables include sample cells, volume reduction rods, filters, O-rings, caps, and weighing platforms necessary for adsorption isotherm measurement. ■ NSD capsules, liquid bottles, sample cells of various sizes, and quick seals are also part of the consumables. *For more details, please refer to the PDF materials or feel free to contact us.

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High-precision gas/vapor adsorption measurement device "BELSORP MAX II"

Demo/Analysis now available. Optimal conditions for each measurement are automatically generated! Anyone can easily achieve accurate isothermal line evaluation in a short time.

The "BELSORP MAX II" is a measurement device that can evaluate specific surface area, pore size distribution, various gas and vapor adsorption amounts, and chemical adsorption amounts with high precision. It enables the evaluation of pore distribution from micropores through adsorption isotherm measurements at very low pressures. It allows for a wide range of surface property evaluations, such as hydrophilicity/hydrophobicity due to organic vapor and water vapor adsorption, and the assessment of surface acidity and basicity. 【Features】 ■ Specific surface area measurement range - 0.01 m²/g or more (N2) - 0.0005 m²/g or more (Kr) ■ Pore distribution measurement range - 0.35 to 500 nm *For more details, please refer to the PDF document or feel free to contact us.

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