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  4. Case study of failure analysis of oxide-based all-solid-state batteries.
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  • Dec 07, 2023
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Dec 07, 2023

Case study of failure analysis of oxide-based all-solid-state batteries.

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We will introduce a case where a series of analyses from failure location identification to cross-sectional observation was conducted on oxide-based all-solid-state batteries that were destroyed by reliability testing. Thermal analysis revealed a tendency for strong heat generation on the side, and X-ray transmission observation showed a white linear contrast anomaly near the boundary where heat generation was observed in the X-ray transmission image. It is suspected that some abnormality may be occurring in the white line area. When CP cross-sectional SEM observation was performed on the area where the anomaly was visible, layer delamination was observed. It is speculated that the positive (negative) electrode layer expanded and contracted repeatedly due to reliability testing, resulting in delamination occurring between the current collector and the electrolyte layer.
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Case study of failure analysis of oxide-based all-solid-state batteries.

It has high safety and can be used in various environments! Consistent analysis is possible.

We present a case study of a series of analyses conducted to identify failure points and perform cross-sectional observations on an oxide-based all-solid-state battery that was destroyed during reliability testing. Thermal analysis revealed a tendency for strong heat generation on the side, and X-ray transmission observations showed white linear contrast anomalies near the boundary where heat generation was observed in the X-ray transmission image. It is suspected that some abnormalities may have occurred in the white line area. When CP cross-sectional SEM observations were conducted on the areas where anomalies were visible, layer delamination was observed. It is inferred that delamination occurred between the current collector and electrolyte layers due to the expansion and contraction of the positive (negative) electrode layers during reliability testing. 【Case Overview】 ■ Sample Information: Oxide-based all-solid-state battery that experienced degradation due to charge and discharge testing ■ Thermal Analysis Results: A tendency for strong heat generation on the side was observed ■ Other Analysis Contents: - X-ray transmission observation - CP cross-sectional observation and elemental analysis via SEM *For more details, please refer to the PDF document or feel free to contact us.

  • Batteries and Capacitors

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Composition analysis of raw materials for all-solid-state batteries.

The purity of the electrolyte greatly affects the performance of the battery! It suppresses the volatility of sulfur components and converts them into a form that can be detected by IC.

We will introduce an example of analyzing the purity of diphosphorus pentasulfide using ion chromatography for the composition analysis of raw materials for all-solid-state batteries. Diphosphorus pentasulfide is one of the raw materials used in the production of electrolytes for sulfide-based all-solid-state batteries. As a pretreatment for IC measurement, the powder of diphosphorus pentasulfide was dissolved in alkaline water and converted into phosphate and sulfide salts. Subsequently, the sulfide ions were oxidized to sulfate ions to prepare the IC measurement solution. For more details, please refer to the published catalog. 【Solid Electrolytes (Partial)】 ■Li3PS4 ■Li7P3S11 ■Li6PS5Cl ■Li6PS5Br *For more information, please refer to the PDF document or feel free to contact us.

  • Analysis and prediction system

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Identification of failure points in electronic components through thermal analysis.

It is possible to perform non-destructive testing from fault location identification to internal observation! High-precision identification of heat generation areas can be achieved.

Thermal analysis is a method for identifying defective areas by detecting the heat generated at leak points due to applied voltage using a high-sensitivity InSb camera. By detecting the weak heat generated from shorts and leaks with a high-sensitivity InSb camera, it is possible to non-destructively identify the failure points of electronic components such as semiconductors. Furthermore, non-destructive observation can also be performed using X-ray inspection equipment. 【Features】 ■ Identifying defective areas by detecting the heat generated at leak points with a high-sensitivity InSb camera ■ Analyzing samples in a non-destructive state, and analyzing electronic components that are difficult to analyze with OBIRCH or emission methods is also possible ■ By using the lock-in function to obtain phase information, it is possible to accurately identify the heat generation points *For more details, please refer to the PDF document or feel free to contact us.

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MLCC crack X-ray observation

Cracks that couldn't be detected visually might be found with X-rays!

When stress such as warping, bending, or twisting is applied to the printed circuit board, cracks may occur inside the MLCC (Multi-Layer Ceramic Chip Capacitor). Moreover, cracks that develop internally are often hidden beneath the electrodes, making it difficult to detect them through visual inspection. In such cases, how about checking with X-rays? [Observation Details] ■ Oblique CT Observation It is possible to perform CT without destroying the printed circuit board, in its original state. ■ Orthogonal CT Observation It is possible to observe the shape of the components in their original state. *For more details, please refer to the PDF document or feel free to contact us.

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Related catalog(4)

Case study of failure analysis of oxide-based all-solid-state batteries.

Case study of failure analysis of oxide-based all-solid-state batteries.

TECHNICAL
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Composition analysis of raw materials for all-solid-state batteries.

Composition analysis of raw materials for all-solid-state batteries.

OTHER
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Identification of failure locations in electronic components through thermal analysis.

Identification of failure locations in electronic components through thermal analysis.

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MLCC crack X-ray observation

MLCC crack X-ray observation

TECHNICAL
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The new product "Vehicle Count Sensor CCS3" enables efficient occupancy management of large parking lots.

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Hotron Inc. has launched its new product, the "Vehicle Count Sensor CCS3"! This product is a ceiling-mounted sensor that combines infrared and radar technology. It reliably detects vehicles in both directions with a single unit, accommodating traffic during congestion and vehicle passing, thus achieving efficient occupancy management in large parking lots. Additionally, it can be utilized for exit warning purposes in addition to vehicle counting, contributing to the safe and smooth operation of parking facilities. 'Features' - Improved detection performance against changes in road surface during rainy weather by using both infrared and radar. - Equipped with IP67 waterproof and dustproof performance, making it effective even in salt damage areas. - Various settings can be configured from a dedicated app (for Android devices), with current settings easily visible at a glance. - The base dimensions are the same as the previous model "CCS2," allowing for smooth replacement of existing equipment. *For more details, please refer to the product information, catalog download, or contact us.*

Oct 30, 2026

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What is a Food Safety Management System (FSMS)?

What is a Food Safety Management System (FSMS)? An explanation of its purpose, benefits, and differences in standards.

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  • OTHER

For food-related businesses, ensuring food safety is an important initiative for enhancing corporate reliability and reducing risks. We provide a clear explanation of the overview of the Food Safety Management System (FSMS), its purpose, expected benefits, and the differences between representative standards such as ISO 22000 and FSSC 22000 in our website's column. If you are considering establishing a food safety framework or obtaining certification, please take a look at the related links.

Oct 30, 2026

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Notice of Participation in SEMICON JAPAN 2026

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We are pleased to announce that we will be exhibiting at "SEMICON JAPAN 2026," which will be held at Tokyo Big Sight from December 9 (Wednesday) to December 11 (Friday). At this exhibition, we will showcase our temperature control devices for semiconductor manufacturing processes, primarily featuring chillers, air conditioning units, and valve products. ▶ Dates: December 9, 2026 (Wednesday) 10:00-17:00 December 10, 2026 (Thursday) 10:00-17:00 December 11, 2026 (Friday) 10:00-17:00 ▶ Venue: Tokyo Big Sight, East Hall 1 (Booth #E1725) We sincerely look forward to your visit.

Oct 30, 2026

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[Publication Announcement] 530 Saiwood Exterior Catalog

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  • CATALOG

We are pleased to announce the release of the latest version of our exterior catalog featuring our artificial wood product "Ayagi." This catalog includes products such as wood decks, fences, balcony railings, and screen louvers. The digital catalog can be viewed through the related link below. Additionally, for customers who wish to receive a printed copy, requests can be made through the materials request page. We hope you find it useful in selecting your products.

Oct 30, 2026

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Announcement of Participation in the 96th Tsukuba Research Seed/Venture Technology Presentation (12/11) - AI for Face Impersonation Detection and Blink Detection

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Swallow Incubate Co., Ltd. will participate in the "96th Tsukuba Research Seed/Venture Technology Presentation" (Theme: Cutting-edge Measurement Technology - Seeing) hosted by the Tsukuba Research Support Center and Tsukuba University on December 11, 2026 (Friday). Our representative director, Toshikazu Ohno, will present on the topic "Protecting and Measuring with the Eyes - AI for Face Impersonation Detection and Blink Detection," introducing two technologies that read the state of the face and eyes from camera footage, as well as how to incorporate them into products and services. ■ Event Overview - Date and Time: December 11, 2026 (Friday) 14:00 - 16:00 - Venue: Tsukuba Research Support Center Training Room A / Online (Zoom Webinar) - Participation Fee: Free - Organized by: Tsukuba Research Support Center / Tsukuba University There will be time for business card exchanges at the on-site venue, and online participants can also apply for individual meetings at a later date. Please refer to the news release in the related links for application details.

Oct 30, 2026

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